Synthese und Kristallstruktur von Pentakis(dimethylsulfoxid)- oxo-titan(IV)chlorid: Herrn Professor Dr. Walter Siebert zum 60. Geburtstag gewidmet = Synthesis and crystal structure of Pentakis(dimethylsulfoxide)-oxo-titanium(IV) chloride
Pentakis(dimethylsulfoxide)-oxo-titanium(IV) chloride is obtained by reaction of titanium tetrachloride with a stoichiometric amount of water in dimethylsulfoxide. A single crystal structure determination (P1̄, a = 9.564(6), b = 10.504(7), c = 12.510(8) Å, α = 70.21(5), β = 83.48(5), γ = 89.82(5)°,...
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| Hauptverfasser: | , , |
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| Dokumenttyp: | Article (Journal) Festschrift |
| Sprache: | Englisch Deutsch |
| Veröffentlicht: |
1997
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| In: |
Zeitschrift für Naturforschung. B, a journal of chemical sciences
Year: 1997, Jahrgang: 52, Heft: 4, Pages: 496-499 |
| ISSN: | 1865-7117 |
| DOI: | 10.1515/znb-1997-0411 |
| Schlagworte: | |
| Online-Zugang: | Verlag, Volltext: http://dx.doi.org/10.1515/znb-1997-0411 Verlag, Volltext: https://www.degruyterbrill.com/view/j/znb.1997.52.issue-4/znb-1997-0411/znb-1997-0411.xml 
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| Verfasserangaben: | M. Enders, R. Rudolph, H. Pritzkow |
MARC
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| 245 | 1 | 0 | |a Synthese und Kristallstruktur von Pentakis(dimethylsulfoxid)- oxo-titan(IV)chlorid |b Herrn Professor Dr. Walter Siebert zum 60. Geburtstag gewidmet = Synthesis and crystal structure of Pentakis(dimethylsulfoxide)-oxo-titanium(IV) chloride |c M. Enders, R. Rudolph, H. Pritzkow |
| 246 | 3 | 1 | |a Synthesis and crystal structure of Pentakis(dimethylsulfoxide)-oxo-titanium(IV) chloride |
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| 520 | |a Pentakis(dimethylsulfoxide)-oxo-titanium(IV) chloride is obtained by reaction of titanium tetrachloride with a stoichiometric amount of water in dimethylsulfoxide. A single crystal structure determination (P1̄, a = 9.564(6), b = 10.504(7), c = 12.510(8) Å, α = 70.21(5), β = 83.48(5), γ = 89.82(5)°, V = 1174 Å3, Z = 2) shows a dicationic titanium(IV) complex with five dimethylsulfoxide ligands and one oxygen atom. The two chlorine anions are not bonded to the complex cation. The TiO6-fragment is a distorted octahedron, where five of the six oxygen atoms belong to the coordinated dimethylsulfoxide molecules. | ||
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