Improving fabrication and application of zach phase plates for phase-contrast transmission electron microscopy
Zach phase plates (PPs) are promising devices to enhance phase contrast in transmission electron microscopy. The Zach PP shifts the phase of the zero-order beam by a strongly localized inhomogeneous electrostatic potential in the back focal plane of the objective lens. We present substantial improve...
Gespeichert in:
| Hauptverfasser: | , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
2012
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| In: |
Microscopy and microanalysis
Year: 2012, Jahrgang: 18, Heft: 5, Pages: 1010-1015$h6 |
| ISSN: | 1435-8115 |
| DOI: | 10.1017/S1431927612001560 |
| Online-Zugang: | Verlag, Volltext: http://dx.doi.org/10.1017/S1431927612001560 Verlag, Volltext: https://www.cambridge.org/core/journals/microscopy-and-microanalysis/article/Improving-fabrication-and-application-of-zach-phase-plates-for-phasecontrast-transmission-electron-microscopy/6D5FB65D7A881D12EB622B03DFD17733 
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| Verfasserangaben: | Simon Hettler, Björn Gamm, Manuel Dries, Nicole Frindt, Rasmus R. Schröder and Dagmar Gerthsen |
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| 520 | |a Zach phase plates (PPs) are promising devices to enhance phase contrast in transmission electron microscopy. The Zach PP shifts the phase of the zero-order beam by a strongly localized inhomogeneous electrostatic potential in the back focal plane of the objective lens. We present substantial improvements of the Zach PP, which overcome previous limitations. The implementation of a microstructured heating device significantly reduces contamination and charging of the PP structure and extends its lifetime. An improved production process allows fabricating PPs with reduced dimensions resulting in lower cut-on frequencies as revealed by simulations of the electrostatic potential. Phase contrast with inversion of PbSe nanoparticles is demonstrated in a standard transmission electron microscope with LaB6 cathode by applying different voltages. | ||
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| 650 | 4 | |a weak-phase object | |
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