Three-legged 2,2′-bipyridine monomer at the air/water interface: monolayer structure and reactions with Ni(II) ions from the subphase
The behavior of compound 2 [1,3,5-tri(2,2′bipyridin-5-yl)benzene] with three bipyridine units arranged in a star geometry is investigated in the presence and absence of Ni(ClO4)2. Its properties at the air−water interface as well as after transfer onto a solid substrate are studied by several techni...
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| Hauptverfasser: | , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
January 26, 2017
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| In: |
Langmuir
Year: 2017, Jahrgang: 33, Heft: 7, Pages: 1646-1654 |
| ISSN: | 1520-5827 |
| DOI: | 10.1021/acs.langmuir.6b04282 |
| Online-Zugang: | Verlag, Volltext: http://dx.doi.org/10.1021/acs.langmuir.6b04282 Verlag, Volltext: http://pubs.acs.org/doi/10.1021/acs.langmuir.6b04282 
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| Verfasserangaben: | Wenyang Dai, Lay-Theng Lee, Andri Schütz, Benjamin Zelenay, Zhikun Zheng, Andreas Borgschulte, Max Döbeli, Wasim Abuillan, Oleg V. Konovalov, Motomu Tanaka, and A. Dieter Schlüter |
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| 245 | 1 | 0 | |a Three-legged 2,2′-bipyridine monomer at the air/water interface |b monolayer structure and reactions with Ni(II) ions from the subphase |c Wenyang Dai, Lay-Theng Lee, Andri Schütz, Benjamin Zelenay, Zhikun Zheng, Andreas Borgschulte, Max Döbeli, Wasim Abuillan, Oleg V. Konovalov, Motomu Tanaka, and A. Dieter Schlüter |
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| 520 | |a The behavior of compound 2 [1,3,5-tri(2,2′bipyridin-5-yl)benzene] with three bipyridine units arranged in a star geometry is investigated in the presence and absence of Ni(ClO4)2. Its properties at the air−water interface as well as after transfer onto a solid substrate are studied by several techniques including Brewster angle microscopy, X-ray reflectivity, neutron reflectivity, X-ray photoelectron spectroscopy, Rutherford backscattering spectrometry, and atomic force microscopy combined with optical microscopy. It is found that compound 2 within the monolayers formed stays almost vertical at the interface and that at high Ni2+/2 (Ni2+/2 = 4000, 20′000) ratios two of the three bipyridine units of 2 are complexed, resulting in supramolecular sheets that are likely composed of arrays of linear metal−organic complexation polymers. | ||
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