2D spherulites of a semi-fluorinated alkane: controlled access to either radial or ring-banded morphologies
Thin films of a semi-fluorinated alkane cast onto solid substrates consist of well-formed two-dimensional non-birefringent ring-banded and/or radial spherulites. Controlling the experimental conditions allows orientation of the crystallization toward either radial-only or ring-banded-only morphologi...
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| Hauptverfasser: | , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
2018
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| In: |
ChemPhysChem
Year: 2017, Jahrgang: 19, Heft: 1, Pages: 29-33 |
| ISSN: | 1439-7641 |
| DOI: | 10.1002/cphc.201701064 |
| Online-Zugang: | Verlag, Volltext: http://dx.doi.org/10.1002/cphc.201701064 Verlag, Volltext: https://onlinelibrary.wiley.com/doi/abs/10.1002/cphc.201701064 
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| Verfasserangaben: | Xianhe Liu, Salomé Mielke, Christophe Contal, Damien Favier, Akihisa Yamamoto, Motomu Tanaka, and Marie Pierre Krafft |
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| 245 | 1 | 0 | |a 2D spherulites of a semi-fluorinated alkane |b controlled access to either radial or ring-banded morphologies |c Xianhe Liu, Salomé Mielke, Christophe Contal, Damien Favier, Akihisa Yamamoto, Motomu Tanaka, and Marie Pierre Krafft |
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| 520 | |a Thin films of a semi-fluorinated alkane cast onto solid substrates consist of well-formed two-dimensional non-birefringent ring-banded and/or radial spherulites. Controlling the experimental conditions allows orientation of the crystallization toward either radial-only or ring-banded-only morphologies. Intermediate states were also captured in which both radial and ring-banded spherulites coexist. Monitoring of the formation of these intermediate states brought evidence for a first crystallization mode that sweeps radially outwards from a central nucleus until the propagating front edge experiences a second crystallization mode that proceeds through a diffusion-controlled rhythmic crystallization mechanism that leads to high (≈2 μm) concentric ridges. These 2D spherulites were investigated by optical and atomic force microscopies, interferometric profilometry, and off-specular neutron scattering. | ||
| 534 | |c 2017 | ||
| 650 | 4 | |a crystallization | |
| 650 | 4 | |a non-birefringence | |
| 650 | 4 | |a polycrystalline aggregates | |
| 650 | 4 | |a self-association | |
| 650 | 4 | |a semi-fluorinated alkanes | |
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