Synthesis and structural characterization of group 10 metal complexes bearing an amidodiphosphine pincer ligand: Dedicated to Prof. Dr. Alexander C. Filippou on the Occasion of his 60th Birthday
Deprotonation of 3,6-di-tert-butyl-1,8-bis((diisopropyl-phosphanyl)-methyl)-9H-carbazole [(CbzdiphosiPr)H] (1) with LiHMDS and reaction with (cod)PtCl2 yielded the corresponding platinum chloride complex (CbzdiphosiPr)PtCl (2), which was converted quantitatively into the bromide 3 and iodide 4 analo...
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| Hauptverfasser: | , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
16 June 2018
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| In: |
Zeitschrift für anorganische und allgemeine Chemie
Year: 2018, Jahrgang: 644, Heft: 17, Pages: 1011-1017 |
| ISSN: | 1521-3749 |
| DOI: | 10.1002/zaac.201800173 |
| Online-Zugang: | Verlag, Volltext: https://doi.org/10.1002/zaac.201800173 Verlag, Volltext: https://onlinelibrary.wiley.com/doi/abs/10.1002/zaac.201800173 
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| Verfasserangaben: | Deborah Hartmann, Hubert Wadepohl, Lutz H. Gade |
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| 245 | 1 | 0 | |a Synthesis and structural characterization of group 10 metal complexes bearing an amidodiphosphine pincer ligand |b Dedicated to Prof. Dr. Alexander C. Filippou on the Occasion of his 60th Birthday |c Deborah Hartmann, Hubert Wadepohl, Lutz H. Gade |
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| 520 | |a Deprotonation of 3,6-di-tert-butyl-1,8-bis((diisopropyl-phosphanyl)-methyl)-9H-carbazole [(CbzdiphosiPr)H] (1) with LiHMDS and reaction with (cod)PtCl2 yielded the corresponding platinum chloride complex (CbzdiphosiPr)PtCl (2), which was converted quantitatively into the bromide 3 and iodide 4 analogues by treatment with TMS-Hal (Hal = Br, I). Moreover, it was possible to prepare a PtIV species by oxidative addition of CsBr3 to compound 3. Furthermore, the hydride complexes of all group 10 metals were obtained by treatment of compound 1 with the M(0) precursors Ni(cod)2, Pd(PtBu3)2, and Pt(PtBu3)2. | ||
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