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A nickel-salphen type complex with a heteropicene backbone

Acenes and heteroacenes as well as other larger fused aromatics and heteroaromatics are per se interesting for organic electronics. Among the large variety of such compounds those annulated π systems that bear multidentate complexation sites for transition metals are rare. This is even more true, th...

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Hauptverfasser: Elbert, Sven (VerfasserIn) , Rominger, Frank (VerfasserIn) , Mastalerz, Michael (VerfasserIn)
Dokumenttyp: Article (Journal)
Sprache:Englisch
Veröffentlicht: 08 May 2018
In: Zeitschrift für anorganische und allgemeine Chemie
Year: 2018, Jahrgang: 644, Heft: 14, Pages: 606-610
ISSN:1521-3749
DOI:10.1002/zaac.201800115
Online-Zugang:Verlag, Volltext: https://doi.org/10.1002/zaac.201800115
Verlag: https://onlinelibrary.wiley.com/doi/abs/10.1002/zaac.201800115
Volltext
Verfasserangaben:Sven M. Elbert, Frank Rominger, Michael Mastalerz

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520 |a Acenes and heteroacenes as well as other larger fused aromatics and heteroaromatics are per se interesting for organic electronics. Among the large variety of such compounds those annulated π systems that bear multidentate complexation sites for transition metals are rare. This is even more true, the larger the π systems are. Picene is an alternating angular annulated π system consisting of five benzene rings. Here, the synthesis of a heteropicene that contains both thiophene and pyridine rings is introduced, whereas the nitrogen atoms are arranged in a phenanthroline subunit to which phenol units are connected, forming a tetradentate ligand. The complexation of NiII by this ligand is described and analysed by single-crystal X-ray diffraction as well as UV/Vis spectroscopy. 
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