The effects of surface conditioning and aging on the bond strength between composite cement and zirconia-reinforced lithium-silicate glass-ceramics

PURPOSE: To determine the effects of ceramic-surface conditioning and aging on the bond strength between composite cement and zirconia-reinforced lithium-silicate glass-ceramics (ZLS) under simulated clinical conditions. - MATERIALS AND METHODS: ZLS disks (Celtra Duo, Dentsply Sirona, n = 110 test g...

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Bibliographic Details
Main Authors: Bömicke, Wolfgang (Author) , Rammelsberg, Peter (Author) , Krisam, Johannes (Author) , Rues, Stefan (Author)
Format: Article (Journal)
Language:English
Published: 2019
In: The journal of adhesive dentistry
Year: 2019, Volume: 21, Issue: 6, Pages: 567-576
ISSN:1757-9988
DOI:10.3290/j.jad.a43650
Online Access:Resolving-System, Volltext: http://doi.org/10.3290/j.jad.a43650
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Author Notes:Wolfgang Bömicke, Peter Rammelsberg, Johannes Krisam, Stefan Rues

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520 |a PURPOSE: To determine the effects of ceramic-surface conditioning and aging on the bond strength between composite cement and zirconia-reinforced lithium-silicate glass-ceramics (ZLS) under simulated clinical conditions. - MATERIALS AND METHODS: ZLS disks (Celtra Duo, Dentsply Sirona, n = 110 test group n = 10, diameter: 8.3 mm, height: 3.4 mm) were assigned to four surface-conditioning groups: (I) 30 s of ~5% hydrofluoric-acid etching (Vita Ceramics Etch, Vita; HF), silanization (Calibra Silane; SIL); (II) successive contamination with saliva and silicone (CONT), HF, SIL; (III) CONT, tribochemical silicatization (CoJet), SIL; (IV) HF, SIL, application and light polymerization of an adhesive (Prime&Bond Active), CONT, reapplication and light polymerization of the adhesive. The ZLS disks were bonded to composite-resin cylinders in acrylic tubes (inner diameter: 3.3 mm) using self-adhesive composite cement (Calibra Universal). The tensile-bond strength (TBS) was measured after both 24 h and 6 months of water storage (WS). Additional aging protocols were tested for group I (3-day WS; 30-day WS including 7500 thermocycles between 6.5 and 60°C; 150-day WS including 37,500 thermocycles). - RESULTS: After 24 h, the mean TBS ranged between 21 MPa (group III) and 30-35 MPa (remaining groups). With the exception of 3-day WS, TBS was statistically significantly reduced by aging. The greatest reduction was observed for silicatized specimens (group III, mean TBS after aging: 9.8 MPa). - CONCLUSION: Both ceramic surface conditioning and aging had a statistically significant effect on the bond strength between composite cement and ZLS. A treatment protocol based on tribochemical silicatization cannot be recommended for the adhesive cementation of ZLS. 
650 4 |a acid etching 
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650 4 |a aging 
650 4 |a air abrasion 
650 4 |a all-ceramic 
650 4 |a bond durability 
650 4 |a Ceramics 
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650 4 |a Composite Resins 
650 4 |a Dental Bonding 
650 4 |a Dental Porcelain 
650 4 |a Lithium 
650 4 |a Materials Testing 
650 4 |a Resin Cements 
650 4 |a Silanes 
650 4 |a Silicates 
650 4 |a Surface Properties 
650 4 |a tensile bond strength 
650 4 |a Tensile Strength 
650 4 |a Zirconium 
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