Cover Image

Practical preparation of cyclopropenone 1,3-propanediol ketal

Cyclopropenone 1,3-propanediol ketal is an increasingly versatile building block for the introduction of various C3 and dioxaspiro units due to the emergence of numerous methodologies for the application of strained hydrocarbons. This Practical Synthetic Procedure gives an updated synthesis for a ba...

Full description

Saved in:
Bibliographic Details
Main Authors: Mulks, Florian (Author) , Heckershoff, Robin (Author) , Zimmer, Marc (Author) , Hashmi, A. Stephen K. (Author)
Format: Article (Journal)
Language:English
Published: 24.02.2020
In: Synthesis
Year: 2020, Volume: 52, Issue: 8, Pages: 1211-1214
ISSN:1437-210X
DOI:10.1055/s-0039-1690830
Online Access:Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1055/s-0039-1690830
Verlag, lizenzpflichtig, Volltext: http://www.thieme-connect.de/DOI/DOI?10.1055/s-0039-1690830
Get full text
Author Notes:Florian F. Mulks, Robin Heckershoff, Marc Zimmer, A. Stephen K. Hashmi
Description
Summary:Cyclopropenone 1,3-propanediol ketal is an increasingly versatile building block for the introduction of various C3 and dioxaspiro units due to the emergence of numerous methodologies for the application of strained hydrocarbons. This Practical Synthetic Procedure gives an updated synthesis for a basic ketal of cyclopropenone with lowered solvent toxicity and a detailed step-by-step guide for the safe production of potassium amide in liquid ammonia and for its application in the synthesis of the cyclopropene ring.
Item Description:Gesehen am 07.05.2020
Physical Description:Online Resource
ISSN:1437-210X
DOI:10.1055/s-0039-1690830

Similar Items