Practical preparation of cyclopropenone 1,3-propanediol ketal
Cyclopropenone 1,3-propanediol ketal is an increasingly versatile building block for the introduction of various C3 and dioxaspiro units due to the emergence of numerous methodologies for the application of strained hydrocarbons. This Practical Synthetic Procedure gives an updated synthesis for a ba...
Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Article (Journal) |
| Language: | English |
| Published: |
24.02.2020
|
| In: |
Synthesis
Year: 2020, Volume: 52, Issue: 8, Pages: 1211-1214 |
| ISSN: | 1437-210X |
| DOI: | 10.1055/s-0039-1690830 |
| Online Access: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1055/s-0039-1690830 Verlag, lizenzpflichtig, Volltext: http://www.thieme-connect.de/DOI/DOI?10.1055/s-0039-1690830 |
| Author Notes: | Florian F. Mulks, Robin Heckershoff, Marc Zimmer, A. Stephen K. Hashmi |
MARC
| LEADER | 00000caa a2200000 c 4500 | ||
|---|---|---|---|
| 001 | 1697661815 | ||
| 003 | DE-627 | ||
| 005 | 20230427190244.0 | ||
| 007 | cr uuu---uuuuu | ||
| 008 | 200507s2020 xx |||||o 00| ||eng c | ||
| 024 | 7 | |a 10.1055/s-0039-1690830 |2 doi | |
| 035 | |a (DE-627)1697661815 | ||
| 035 | |a (DE-599)KXP1697661815 | ||
| 035 | |a (OCoLC)1341319249 | ||
| 040 | |a DE-627 |b ger |c DE-627 |e rda | ||
| 041 | |a eng | ||
| 084 | |a 30 |2 sdnb | ||
| 100 | 1 | |a Mulks, Florian |d 1989- |e VerfasserIn |0 (DE-588)114064971X |0 (DE-627)898621216 |0 (DE-576)493968318 |4 aut | |
| 245 | 1 | 0 | |a Practical preparation of cyclopropenone 1,3-propanediol ketal |c Florian F. Mulks, Robin Heckershoff, Marc Zimmer, A. Stephen K. Hashmi |
| 264 | 1 | |c 24.02.2020 | |
| 300 | |a 4 | ||
| 336 | |a Text |b txt |2 rdacontent | ||
| 337 | |a Computermedien |b c |2 rdamedia | ||
| 338 | |a Online-Ressource |b cr |2 rdacarrier | ||
| 500 | |a Gesehen am 07.05.2020 | ||
| 520 | |a Cyclopropenone 1,3-propanediol ketal is an increasingly versatile building block for the introduction of various C3 and dioxaspiro units due to the emergence of numerous methodologies for the application of strained hydrocarbons. This Practical Synthetic Procedure gives an updated synthesis for a basic ketal of cyclopropenone with lowered solvent toxicity and a detailed step-by-step guide for the safe production of potassium amide in liquid ammonia and for its application in the synthesis of the cyclopropene ring. | ||
| 700 | 1 | |a Heckershoff, Robin |d 1982- |e VerfasserIn |0 (DE-588)1209703858 |0 (DE-627)1697661270 |4 aut | |
| 700 | 1 | |a Zimmer, Marc |e VerfasserIn |0 (DE-588)1179489357 |0 (DE-627)1067389962 |0 (DE-576)518261115 |4 aut | |
| 700 | 1 | |a Hashmi, A. Stephen K. |d 1963- |e VerfasserIn |0 (DE-588)101199576X |0 (DE-627)704823926 |0 (DE-576)169176665 |4 aut | |
| 773 | 0 | 8 | |i Enthalten in |t Synthesis |d Stuttgart [u.a.] : Thieme, 1969 |g 52(2020), 8, Seite 1211-1214 |h Online-Ressource |w (DE-627)324958609 |w (DE-600)2033062-5 |w (DE-576)109293452 |x 1437-210X |7 nnas |a Practical preparation of cyclopropenone 1,3-propanediol ketal |
| 773 | 1 | 8 | |g volume:52 |g year:2020 |g number:8 |g pages:1211-1214 |g extent:4 |a Practical preparation of cyclopropenone 1,3-propanediol ketal |
| 856 | 4 | 0 | |u https://doi.org/10.1055/s-0039-1690830 |x Verlag |x Resolving-System |z lizenzpflichtig |3 Volltext |
| 856 | 4 | 0 | |u http://www.thieme-connect.de/DOI/DOI?10.1055/s-0039-1690830 |x Verlag |z lizenzpflichtig |3 Volltext |
| 951 | |a AR | ||
| 992 | |a 20200507 | ||
| 993 | |a Article | ||
| 994 | |a 2020 | ||
| 998 | |g 101199576X |a Hashmi, A. Stephen K. |m 101199576X:Hashmi, A. Stephen K. |d 120000 |d 120100 |e 120000PH101199576X |e 120100PH101199576X |k 0/120000/ |k 1/120000/120100/ |p 4 |y j | ||
| 998 | |g 1179489357 |a Zimmer, Marc |m 1179489357:Zimmer, Marc |d 120000 |d 120100 |e 120000PZ1179489357 |e 120100PZ1179489357 |k 0/120000/ |k 1/120000/120100/ |p 3 | ||
| 998 | |g 1209703858 |a Heckershoff, Robin |m 1209703858:Heckershoff, Robin |d 500000 |d 501249 |e 500000PH1209703858 |e 501249PH1209703858 |k 0/500000/ |k 1/500000/501249/ |p 2 | ||
| 998 | |g 114064971X |a Mulks, Florian |m 114064971X:Mulks, Florian |p 1 |x j | ||
| 999 | |a KXP-PPN1697661815 |e 3662253372 | ||
| BIB | |a Y | ||
| SER | |a journal | ||
| JSO | |a {"type":{"bibl":"article-journal","media":"Online-Ressource"},"relHost":[{"disp":"Practical preparation of cyclopropenone 1,3-propanediol ketalSynthesis","titleAlt":[{"title":"international journal of synthetic organic chemistry"}],"part":{"pages":"1211-1214","issue":"8","extent":"4","volume":"52","text":"52(2020), 8, Seite 1211-1214","year":"2020"},"id":{"issn":["1437-210X"],"doi":["10.1055/s-00000084"],"eki":["324958609"],"zdb":["2033062-5"]},"title":[{"subtitle":"journal of synthetic organic chemistry","title_sort":"Synthesis","title":"Synthesis"}],"physDesc":[{"extent":"Online-Ressource"}],"type":{"media":"Online-Ressource","bibl":"periodical"},"note":["Gesehen am 07.11.2013"],"language":["eng"],"recId":"324958609","origin":[{"publisher":"Thieme","dateIssuedDisp":"1969-","dateIssuedKey":"1969","publisherPlace":"Stuttgart [u.a.]"}],"pubHistory":["[1.]1969 - [43.]2011; 44.2012 -"]}],"physDesc":[{"extent":"4 S."}],"title":[{"title_sort":"Practical preparation of cyclopropenone 1,3-propanediol ketal","title":"Practical preparation of cyclopropenone 1,3-propanediol ketal"}],"id":{"eki":["1697661815"],"doi":["10.1055/s-0039-1690830"]},"person":[{"display":"Mulks, Florian","family":"Mulks","given":"Florian","role":"aut"},{"role":"aut","given":"Robin","family":"Heckershoff","display":"Heckershoff, Robin"},{"given":"Marc","role":"aut","display":"Zimmer, Marc","family":"Zimmer"},{"display":"Hashmi, A. Stephen K.","family":"Hashmi","given":"A. Stephen K.","role":"aut"}],"origin":[{"dateIssuedKey":"2020","dateIssuedDisp":"24.02.2020"}],"language":["eng"],"recId":"1697661815","note":["Gesehen am 07.05.2020"],"name":{"displayForm":["Florian F. Mulks, Robin Heckershoff, Marc Zimmer, A. Stephen K. Hashmi"]}} | ||
| SRT | |a MULKSFLORIPRACTICALP2402 | ||