Synthesis of triphenylene-based triptycenes via Suzuki-Miyaura cross-coupling and subsequent Scholl reaction
A two-step method (Suzuki-Miyaura cross-coupling, followed by Scholl oxidation) to triphenylene-based triptycenes is described, rendering a variety of π-extended triptycenes accessible in high yields and without the necessity of column chromatography purification. The versatility of this reaction ha...
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| Hauptverfasser: | , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
August 20, 2015
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| In: |
The journal of organic chemistry
Year: 2015, Jahrgang: 80, Heft: 18, Pages: 9342-9348 |
| ISSN: | 1520-6904 |
| DOI: | 10.1021/acs.joc.5b01520 |
| Online-Zugang: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1021/acs.joc.5b01520
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| Verfasserangaben: | Dennis Reinhard, Frank Rominger, and Michael Mastalerz (Organisch-Chemisches Institut, Ruprecht-Karls-Universität Heidelberg) |
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| 520 | |a A two-step method (Suzuki-Miyaura cross-coupling, followed by Scholl oxidation) to triphenylene-based triptycenes is described, rendering a variety of π-extended triptycenes accessible in high yields and without the necessity of column chromatography purification. The versatility of this reaction has been demonstrated in the synthesis of a supertriptycene in only four steps and high yields. | ||
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