Synthesis of alkynylated benzo[a]naphtho[2,3-i]phenazine derivatives
Thermal condensation of 2,3-diamino-1,4-(bistriisopropylsilylethynyl)benzene, -naphthalene,-anthracene, and -benzothiadiazole substrates with 1,2-naphthalenedione forms bent benzophenazine-type heteroarenes in a one-step reaction in good to excellent yields. The targets are investigated by UV/Vis sp...
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| Hauptverfasser: | , , , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
2016
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| In: |
Chemistry - a European journal
Year: 2015, Jahrgang: 22, Heft: 3, Pages: 869-873 |
| ISSN: | 1521-3765 |
| DOI: | 10.1002/chem.201503856 |
| Online-Zugang: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1002/chem.201503856 Verlag, lizenzpflichtig, Volltext: https://chemistry-europe.onlinelibrary.wiley.com/doi/abs/10.1002/chem.201503856 
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| Verfasserangaben: | Sebastian Hahn, Philipp Biegger, Markus Bender, Frank Rominger, and Uwe H.F. Bunz |
MARC
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| 520 | |a Thermal condensation of 2,3-diamino-1,4-(bistriisopropylsilylethynyl)benzene, -naphthalene,-anthracene, and -benzothiadiazole substrates with 1,2-naphthalenedione forms bent benzophenazine-type heteroarenes in a one-step reaction in good to excellent yields. The targets are investigated by UV/Vis spectroscopy, cyclic voltammetry, and single-crystal X-ray crystallography. The packing of the targets in the solid state follows either a herringbone or a brick wall motif. In the case of 8,13-bis(triisopropylsilylethynyl)dibenzo[a,i]phenazine, polymorphs with either packing result. | ||
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