Weak intramolecular C-H⋯H-B and C-H⋯Cl interactions in C-aminoboryl-o-carboranes
Reactions of dilithio-o-carborane Li2C2B10H10 (generated in situ from o-carborane 1 and butyllithium) with aminodichloroboranes R2NBCl2 (R = Et, iPr) led to the corresponding mono- and/or bis-C-aminoboryl-o-carboranes. The molecular compositions of the new o-carborane derivatives follow from NMR and...
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| Hauptverfasser: | , , , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
21 March 2013
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| In: |
Journal of organometallic chemistry
Year: 2013, Jahrgang: 747, Pages: 174-177 |
| ISSN: | 1872-8561 |
| DOI: | 10.1016/j.jorganchem.2013.03.016 |
| Online-Zugang: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1016/j.jorganchem.2013.03.016 Verlag, lizenzpflichtig, Volltext: https://www.sciencedirect.com/science/article/pii/S0022328X13002015 
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| Verfasserangaben: | Yong Nie, Jinling Miao, Hans Pritzkow, Hubert Wadepohl, Walter Siebert |
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| 520 | |a Reactions of dilithio-o-carborane Li2C2B10H10 (generated in situ from o-carborane 1 and butyllithium) with aminodichloroboranes R2NBCl2 (R = Et, iPr) led to the corresponding mono- and/or bis-C-aminoboryl-o-carboranes. The molecular compositions of the new o-carborane derivatives follow from NMR and MS data as well as from X-ray diffraction analyses. The structures of the new carborane compounds feature combined weak intramolecular C-H⋯H-B hydrogen-hydrogen and C-H⋯Cl hydrogen-chlorine bonding in the solid state. | ||
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