Morphology and agglomeration control of LiMnPO4 micro- and nanocrystals
Microwave-assisted hydrothermal synthesis was used to grow LiMnPO4 micro- and nanocrystals from acetate precursors. By appropriate adjustment of the precursor concentration and the pH-value of the reactant, the product composition and purity along with the crystal size can be manipulated, resulting...
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| Hauptverfasser: | , , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
May 21, 2013
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| In: |
Langmuir
Year: 2013, Jahrgang: 29, Heft: 25, Pages: 8054-8060 |
| ISSN: | 1520-5827 |
| DOI: | 10.1021/la3046498 |
| Online-Zugang: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1021/la3046498
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| Verfasserangaben: | Christoph Neef, Carsten Jähne, Hans-Peter Meyer, and Rüdiger Klingeler |
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| 520 | |a Microwave-assisted hydrothermal synthesis was used to grow LiMnPO4 micro- and nanocrystals from acetate precursors. By appropriate adjustment of the precursor concentration and the pH-value of the reactant, the product composition and purity along with the crystal size can be manipulated, resulting in particle-dimensions from around 10 μm down to a few 100 nm. Prisms and plates with hexagonal basal faces as well as cuboid and rod-like particles were produced. The effects on the crystal morphology as well as on the materials texture and agglomeration tendency are discussed and a comprehensive agglomeration phase diagram is constructed. | ||
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