Single crystal growth and physical properties of superconducting ferro-pnictides Ba(Fe, Co)2As2 grown using self-flux and Bridgman techniques
We have employed the high temperature solutions growth technique and the Bridgman technique to grow cm-size high-quality single crystals of pristine BaFe2As2 (Ba122) and its Co-doped superconducting variants. In the first approach, self-flux (Fe, Co)As was used to achieve a homogeneous melt of compo...
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| Hauptverfasser: | , , , , , , , , , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
2011
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| In: |
Journal of crystal growth
Year: 2011, Jahrgang: 314, Heft: 1, Pages: 341-348 |
| DOI: | 10.1016/j.jcrysgro.2010.11.149 |
| Online-Zugang: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1016/j.jcrysgro.2010.11.149 Verlag, lizenzpflichtig, Volltext: https://www.sciencedirect.com/science/article/pii/S0022024810011309 |
| Verfasserangaben: | S. Aswartham, C. Nacke, G. Friemel, N. Leps, S. Wurmehl, N. Wizent, C. Hess, R. Klingeler, G. Behr, S. Singh, B. Büchner |
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| 245 | 1 | 0 | |a Single crystal growth and physical properties of superconducting ferro-pnictides Ba(Fe, Co)2As2 grown using self-flux and Bridgman techniques |c S. Aswartham, C. Nacke, G. Friemel, N. Leps, S. Wurmehl, N. Wizent, C. Hess, R. Klingeler, G. Behr, S. Singh, B. Büchner |
| 246 | 3 | 3 | |a Single crystal growth and physical properties of superconducting ferro-pnictides Ba(Fe, Co) 2 As 2 |
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| 500 | |a Gesehen am 23.03.2022 | ||
| 520 | |a We have employed the high temperature solutions growth technique and the Bridgman technique to grow cm-size high-quality single crystals of pristine BaFe2As2 (Ba122) and its Co-doped superconducting variants. In the first approach, self-flux (Fe, Co)As was used to achieve a homogeneous melt of composition Ba(Fe, Co)3.1As3.1 at T=1463K. The melt was then cooled slowly under a temperature gradient in a double-wall crucible assembly to obtain large and flux-free single crystals of Ba(Fe, Co)2As2. In the second approach, single crystals were grown directly from a stoichiometric Ba(Fe, Co)2As2 melt at T=1723K employing the Bridgman technique associated with a vertical tube furnace. Using both techniques single crystals with lateral dimensions up to 25×10mm2 and thickness up to 1mm were obtained. Details of the two methods are given and a comparative study of the magnetic and transport properties of the single crystals obtained using the two methods is presented. | ||
| 650 | 4 | |a A1. Crystal morphology | |
| 650 | 4 | |a A2. Bridgman technique | |
| 650 | 4 | |a A2. Growth from high temperature solutions | |
| 650 | 4 | |a B1. Ferro-pnictides | |
| 650 | 4 | |a B2. Superconducting materials | |
| 700 | 1 | |a Nacke, C. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Friemel, G. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Leps, N. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Wurmehl, S. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Wizent, N. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Hess, C. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Klingeler, Rüdiger |d 1969- |e VerfasserIn |0 (DE-588)128948736 |0 (DE-627)38613720X |0 (DE-576)187850720 |4 aut | |
| 700 | 1 | |a Behr, G. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Singh, S. |e VerfasserIn |4 aut | |
| 700 | 1 | |a Büchner, B. |e VerfasserIn |4 aut | |
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