Synthesis and characterization of the nido-platinaborane 7,7-(PPh3)2-7-PtB10H11-11-OC(O)Me
The reaction of closo-B 10 H 10 2− with PtCl 2 (PPh 3 ) 2 in the presence of MeCOSH afforded the title platinaborane nido-7,7-(PPh 3 ) 2 -7-PtB 10 H 11 -11-OC(O)Me (1), which has been characterized by IR and NMR spectroscopy, MS, elemental analysis, and single-crystal X-ray diffraction. In contrast...
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| Hauptverfasser: | , , , , , , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
2011
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| In: |
Zeitschrift für Naturforschung. B, a journal of chemical sciences
Year: 2011, Jahrgang: 66, Heft: 4, Pages: 387-391 |
| ISSN: | 1865-7117 |
| DOI: | 10.1515/znb-2011-0408 |
| Online-Zugang: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1515/znb-2011-0408 Verlag, lizenzpflichtig, Volltext: https://www.degruyterbrill.com/document/doi/10.1515/znb-2011-0408/html 
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| Verfasserangaben: | Jinling Miao, Yong Nie, Haiyan Chen, Daqi Wang, Markus Enders, Walter Siebert, Guoxin Sun, and Jianmin Dou |
MARC
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| 245 | 1 | 0 | |a Synthesis and characterization of the nido-platinaborane 7,7-(PPh3)2-7-PtB10H11-11-OC(O)Me |c Jinling Miao, Yong Nie, Haiyan Chen, Daqi Wang, Markus Enders, Walter Siebert, Guoxin Sun, and Jianmin Dou |
| 246 | 3 | 3 | |a Synthesis and characterization of the nido-platinaborane 7,7-(PPh 3) 2 -7-PtB 10 H 11 -11-OC(O)Me |
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| 500 | |a Im Titel sind die Zahlen 3, 2, 10 und 11 tiefgestellt | ||
| 500 | |a Gesehen am 19.08.2022 | ||
| 520 | |a The reaction of closo-B 10 H 10 2− with PtCl 2 (PPh 3 ) 2 in the presence of MeCOSH afforded the title platinaborane nido-7,7-(PPh 3 ) 2 -7-PtB 10 H 11 -11-OC(O)Me (1), which has been characterized by IR and NMR spectroscopy, MS, elemental analysis, and single-crystal X-ray diffraction. In contrast to the known products having exo-polyhedral Pt-S-C-O-B ring(s) from the same reaction with Ph- COSH, compound 1 has a B-acetoxy group on the open PtB 4 face of the nido-PtB 10 cluster. The structure of 1 features both intramolecular/intermolecular C-H· · ·O hydrogen bonds and intramolecular C-H· · ·H-B dihydrogen bonds, which link the molecules into a 1-D chain structure. Graphical Abstract Synthesis and Characterization of the nido-Platinaborane 7,7-(PPh3)2-7-PtB 10 H 11 -11-OC(O)Me | ||
| 650 | 4 | |a Boron Cluster | |
| 650 | 4 | |a Hydrogen Bond | |
| 650 | 4 | |a Metallaborane | |
| 650 | 4 | |a Platinaborane | |
| 650 | 4 | |a Supramolecular Chemistry | |
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| 700 | 1 | |a Dou, Jianmin |e VerfasserIn |4 aut | |
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