Benchmarking mechanical properties of 3D printed elastomeric microstructures [data]

The characterization of mechanical properties in soft 3D printed materials at the microscale remains a significant challenge due to the lack of standardized methodologies. To address this issue, a microscale nanoindentation protocol for elastomeric 3D printed microstructures is developed, optimized,...

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Hauptverfasser: Eivgi, Or (VerfasserIn) , Vázquez-Martel, Clara (VerfasserIn) , Lukeš, Jaroslav (VerfasserIn) , Blasco, Eva (VerfasserIn)
Dokumenttyp: Datenbank Forschungsdaten
Sprache:Englisch
Veröffentlicht: Heidelberg Universität 2025-05-09
DOI:10.11588/DATA/4OZZTW
Schlagworte:
Online-Zugang:Verlag, kostenfrei, Volltext: https://doi.org/10.11588/DATA/4OZZTW
Verlag, kostenfrei, Volltext: https://heidata.uni-heidelberg.de/dataset.xhtml?persistentId=doi:10.11588/DATA/4OZZTW
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Verfasserangaben:Or Eivgi, Clara Vazquez-Martel, Jaroslav Lukeš, Eva Blasco

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520 |a The characterization of mechanical properties in soft 3D printed materials at the microscale remains a significant challenge due to the lack of standardized methodologies. To address this issue, a microscale nanoindentation protocol for elastomeric 3D printed microstructures is developed, optimized, and benchmarked. Herein, a conospherical indenter tip (r = 10.26 µm), a modified trapezoidal displacement profile with lift-off segments to capture adhesion interactions, and the nano-Johnson-Kendall-Roberts model for data analysis are employed. The protocol is optimized and verified using four newly developed PDMS-based inks for two-photon 3D laser printing. The results are compared to a state-of-the-art literature protocol that uses a Berkovich tip and the Oliver-Pharr model. It is shown that adhesion forces play a significant role in mechanical properties overestimation, showing differences of up to 80% between the different protocols. This study highlights the importance of carefully selecting characterization protocol to yield comparable results between studies. By providing a standardized protocol, it paves the way for straightforward and accurate characterization of mechanical properties in soft 3D printed materials at the microscale. 
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