Highly substituted medium-sized ring-fused azocinoquinoline scaffolds by post-Ugi-4CR reductive carbopalladation cyclization
A concise synthesis of quinoline-fused eight-membered rings from simple starting materials is described. Reductive cyclo-carbopalladation of suitable Ugi-4CR substrates as a key step leads to the regio- and diastereoselective formation of 1,2-dihydroazocino[4,3-b]quinolin-3-ones under mild reaction...
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| Hauptverfasser: | , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
July 30, 2019
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| In: |
The journal of organic chemistry
Year: 2019, Jahrgang: 84, Heft: 17, Pages: 10740-10748 |
| ISSN: | 1520-6904 |
| DOI: | 10.1021/acs.joc.9b01269 |
| Online-Zugang: | Verlag, Volltext: https://doi.org/10.1021/acs.joc.9b01269
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| Verfasserangaben: | Helya Janatian Ghazvini, Thomas J. J. Müller, Frank Rominger, and Saeed Balalaie |
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| 520 | |a A concise synthesis of quinoline-fused eight-membered rings from simple starting materials is described. Reductive cyclo-carbopalladation of suitable Ugi-4CR substrates as a key step leads to the regio- and diastereoselective formation of 1,2-dihydroazocino[4,3-b]quinolin-3-ones under mild reaction conditions with good yields in short reaction time. | ||
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