Size matters: radiocarbon dates of <200 [mu]g ancient collagen samples with AixMICADAS and its gas ion source

For many of archaeology’s rarest and most enigmatic bone artifacts (e.g. human remains, bone ornaments, worked bone), the destruction of the 500 mg material necessary for direct accelerator mass spectrometry (AMS) dating on graphite targets would cause irreparable damage; therefore many have not bee...

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Main Authors: Fewlass, Helen (Author) , Talamo, Sahra (Author) , Tuna, Thibaut (Author) , Fagault, Yoann (Author) , Kromer, Bernd (Author) , Hoffmann, Helene (Author) , Pangrazzi, Caterina (Author) , Hublin, Jean-Jacques (Author) , Bard, Edouard (Author)
Format: Article (Journal)
Language:English
Published: 2018
In: Radiocarbon
Year: 2017, Volume: 60, Issue: 2, Pages: 425-439
ISSN:1945-5755
DOI:10.1017/RDC.2017.98
Online Access:Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1017/RDC.2017.98
Verlag, lizenzpflichtig, Volltext: https://www.cambridge.org/core/journals/radiocarbon/article/size-matters-radiocarbon-dates-of-200-g-ancient-collagen-samples-with-aixmicadas-and-its-gas-ion-source/5C009537A4A0E1F9CAF0A32C9B60CC4E
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Author Notes:Helen Fewlass, Sahra Talamo, Thibaut Tuna, Yoann Fagault, Bernd Kromer, Helene Hoffmann, Caterina Pangrazzi, Jean-Jacques Hublin, Edouard Bard
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Summary:For many of archaeology’s rarest and most enigmatic bone artifacts (e.g. human remains, bone ornaments, worked bone), the destruction of the 500 mg material necessary for direct accelerator mass spectrometry (AMS) dating on graphite targets would cause irreparable damage; therefore many have not been directly dated. The recently improved gas ion source of the MICADAS (MIni CArbon DAting System) offers a solution to this problem by measuring gaseous samples of 5-100 µg carbon at a level of precision not previously achieved with an AMS gas ion source. We present the results of the first comparison between “routine” graphite dates of ca. 1000 µg C (2-3 mg bone collagen) and dates from aliquots of gaseous samples of <100 µg C (<0.2 mg bone collagen), undertaken with the highest possible precision in mind. The experiment demonstrates the performance of the AixMICADAS in achieving reliable radiocarbon measurements from <0.2 mg collagen samples back to 40,000 14C BP. The technique has great implications for resolving chronological questions for key archaeological artifacts.
Item Description:Published online by Cambridge University Press: 07 November 2017
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Physical Description:Online Resource
ISSN:1945-5755
DOI:10.1017/RDC.2017.98