Efficient, scalable syntheses of important intermediates in tribenzotriquinacene chemistry
<p>A new synthetic procedure for the synthesis of 1,4,7-tribromo-10-methyltribenzotriquinacene on multigram scale is reported. Its conversion into 1,4,7-trimethoxy-10-methyltribenzotriquinacene is also described. Both procedures are simpler and greener alternatives to the known ones, and the c...
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| Hauptverfasser: | , , |
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| Dokumenttyp: | Article (Journal) |
| Sprache: | Englisch |
| Veröffentlicht: |
02.10.2015
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| In: |
Synthesis
Year: 2015, Jahrgang: 47, Heft: 24, Pages: 3846-3848 |
| ISSN: | 1437-210X |
| DOI: | 10.1055/s-0035-1560710 |
| Online-Zugang: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1055/s-0035-1560710 Verlag, lizenzpflichtig, Volltext: http://www.thieme-connect.de/DOI/DOI?10.1055/s-0035-1560710 
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| Verfasserangaben: | Daniel Beaudoin, Frank Rominger, Michael Mastalerz |
| Zusammenfassung: | <p>A new synthetic procedure for the synthesis of 1,4,7-tribromo-10-methyltribenzotriquinacene on multigram scale is reported. Its conversion into 1,4,7-trimethoxy-10-methyltribenzotriquinacene is also described. Both procedures are simpler and greener alternatives to the known ones, and the crystal structures of both compounds are disclosed.</p> |
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| Beschreibung: | Gesehen am 03.08.2020 |
| Beschreibung: | Online Resource |
| ISSN: | 1437-210X |
| DOI: | 10.1055/s-0035-1560710 |