Efficient, scalable syntheses of important intermediates in tribenzotriquinacene chemistry
<p>A new synthetic procedure for the synthesis of 1,4,7-tribromo-10-methyltribenzotriquinacene on multigram scale is reported. Its conversion into 1,4,7-trimethoxy-10-methyltribenzotriquinacene is also described. Both procedures are simpler and greener alternatives to the known ones, and the c...
Saved in:
| Main Authors: | , , |
|---|---|
| Format: | Article (Journal) |
| Language: | English |
| Published: |
02.10.2015
|
| In: |
Synthesis
Year: 2015, Volume: 47, Issue: 24, Pages: 3846-3848 |
| ISSN: | 1437-210X |
| DOI: | 10.1055/s-0035-1560710 |
| Online Access: | Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1055/s-0035-1560710 Verlag, lizenzpflichtig, Volltext: http://www.thieme-connect.de/DOI/DOI?10.1055/s-0035-1560710 
|
| Author Notes: | Daniel Beaudoin, Frank Rominger, Michael Mastalerz |
| Summary: | <p>A new synthetic procedure for the synthesis of 1,4,7-tribromo-10-methyltribenzotriquinacene on multigram scale is reported. Its conversion into 1,4,7-trimethoxy-10-methyltribenzotriquinacene is also described. Both procedures are simpler and greener alternatives to the known ones, and the crystal structures of both compounds are disclosed.</p> |
|---|---|
| Item Description: | Gesehen am 03.08.2020 |
| Physical Description: | Online Resource |
| ISSN: | 1437-210X |
| DOI: | 10.1055/s-0035-1560710 |