Core level photoionization on free sub-10-nm nanoparticles using synchrotron radiation

A novel instrument is presented, which permits studies on singly charged free nanoparticles in the diameter range from 1 to 30 nm using synchrotron radiation in the soft x-ray regime. It consists of a high pressure nanoparticle source, a high efficiency nanoparticle beam inlet, and an electron time-...

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Main Authors: Meinen, Jan (Author) , Khasminskaya, Svetlana (Author) , Eritt, Markus (Author) , Leisner, Thomas (Author) , Antonsson, Egill (Author) , Langer, Burkhard (Author) , Rühl, Eckart (Author)
Format: Article (Journal)
Language:English
Published: 26 August 2010
In: Review of scientific instruments
Year: 2010, Volume: 81, Issue: 8, Pages: 1-4
ISSN:1089-7623
DOI:10.1063/1.3475154
Online Access:Verlag, lizenzpflichtig, Volltext: https://doi.org/10.1063/1.3475154
Verlag, lizenzpflichtig, Volltext: https://aip.scitation.org/doi/10.1063/1.3475154
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Author Notes:Jan Meinen, Svetlana Khasminskaya, Markus Eritt, Thomas Leisner, Egill Antonsson, Burkhard Langer, and Eckart Rühl
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Summary:A novel instrument is presented, which permits studies on singly charged free nanoparticles in the diameter range from 1 to 30 nm using synchrotron radiation in the soft x-ray regime. It consists of a high pressure nanoparticle source, a high efficiency nanoparticle beam inlet, and an electron time-of-flight spectrometer suitable for probing surface and bulk properties of free, levitated nanoparticles. We show results from x-ray photoelectron spectroscopy study near the - Si  - L - 3,2 - Si L3,2 - -edge on 8.2 nm - SiO - 2 - SiO2 - particles prepared in a nanoparticle beam. The possible use of this apparatus regarding chemical reactions on the surface of nanometer-sized particles is highlighted. This approach has the potential to be exploited for process studies on heterogeneous atmospheric chemistry.
Item Description:Gesehen am 13.04.2023
Physical Description:Online Resource
ISSN:1089-7623
DOI:10.1063/1.3475154